n x n Latin Square Design 1 Response var. : Effect of catalyst on the reaction of a chemical process Treatment : Five different catalysts (batches) Block: Days Obs BATCH DAY CATALYST REACTIME 1 1 1 A 8 2 1 2 B 7 3 1 3 D 1 4 1 4 C 7 5 1 5 E 3 6 2 1 C 11 7 2 2 E 2 8 2 3 A 7 9 2 4 D 3 10 2 5 B 8 11 3 1 B 4 12 3 2 A 9 13 3 3 C 10 14 3 4 E 1 15 3 5 D 5 16 4 1 D 6 17 4 2 C 8 18 4 3 E 6 19 4 4 B 6 20 4 5 A 10 21 5 1 E 4 22 5 2 D 2 23 5 3 B 3 24 5 4 A 8 25 5 5 C 8 n x n Latin Square Design 2 Response var. : Effect of catalyst on the reaction of a chemical process Treatment : Five different catalysts (batches) Block: Days ------------------------------------------------------------------------ | | DAY | | |---------------------------------------------------| | | 1 | 2 | 3 | 4 | | |------------+------------+------------+------------| | | REACTIME | REACTIME | REACTIME | REACTIME | | |------------+------------+------------+------------| | | Y(IJ) | Y(IJ) | Y(IJ) | Y(IJ) | |------------------+------------+------------+------------+------------| |BATCH | | | | | |------------------| | | | | |1 | 8.00| 7.00| 1.00| 7.00| |------------------+------------+------------+------------+------------| |2 | 11.00| 2.00| 7.00| 3.00| |------------------+------------+------------+------------+------------| |3 | 4.00| 9.00| 10.00| 1.00| |------------------+------------+------------+------------+------------| |4 | 6.00| 8.00| 6.00| 6.00| |------------------+------------+------------+------------+------------| |5 | 4.00| 2.00| 3.00| 8.00| ------------------------------------------------------------------------ (Continued) --------------------------------- | | DAY | | |------------| | | 5 | | |------------| | | REACTIME | | |------------| | | Y(IJ) | |------------------+------------| |BATCH | | |------------------| | |1 | 3.00| |------------------+------------| |2 | 8.00| |------------------+------------| |3 | 5.00| |------------------+------------| |4 | 10.00| |------------------+------------| |5 | 8.00| --------------------------------- n x n Latin Square Design 3 Response var. : Effect of catalyst on the reaction of a chemical process Treatment : Five different catalysts (batches) Block: Days The ANOVA Procedure Class Level Information Class Levels Values BATCH 5 1 2 3 4 5 DAY 5 1 2 3 4 5 CATALYST 5 A B C D E Number of observations 25 n x n Latin Square Design 4 Response var. : Effect of catalyst on the reaction of a chemical process Treatment : Five different catalysts (batches) Block: Days The ANOVA Procedure Dependent Variable: REACTIME Sum of Source DF Squares Mean Square F Value Pr > F Model 12 169.1200000 14.0933333 4.51 0.0072 Error 12 37.5200000 3.1266667 Corrected Total 24 206.6400000 R-Square Coeff Var Root MSE REACTIME Mean 0.818428 30.07208 1.768238 5.880000 Source DF Anova SS Mean Square F Value Pr > F BATCH 4 15.4400000 3.8600000 1.23 0.3476 DAY 4 12.2400000 3.0600000 0.98 0.4550 CATALYST 4 141.4400000 35.3600000 11.31 0.0005